Patents

US 9758905 B2: Process of making carbon fibers derived from lignin/carbon residue

Granted
2017-09-12
Filed
2013-11-05 application 14440411
Type
Utility · 19 claims
Elsewhere
Google Patents ↗ · USPTO patent document ↗ · USPTO Patent Center record ↗

Abstract

A method of making a carbon fiber comprising esterification of a lignin precursor with an acid, acid anhydride, or acyl halide, thereby forming a reduced Tg lignin. Mixing the reduced Tg lignin with a carbon residue selected from the group of coal based raw material, petroleum based raw material and combinations thereof, thereby forming a fiber precursor mixture; and spinning the fiber precursor mixture into a fiber. A method of making a carbon fiber comprising esterification of a lignin with an acid derivative, thereby forming a reduced Tg lignin. Mixing the reduced Tg lignin with a pitch, thereby forming a fiber precursor mixture; and spinning the fiber precursor mixture into a fiber. A method of making a carbon fiber comprising lowering the Tg of a lignin material, thereby forming a reduced Tg lignin. Mixing the reduced Tg lignin with a carbon residue, thereby forming a fiber precursor mixture and spinning the fiber precursor mixture into a fiber.

Source: PVGPATDIS, file of 2026-04-10 (ipg170912.xml).

Assignees

AssigneeTypePlaceAlso on furp.orgSource
GrafTech International Holdings Inc. 65 patentsUS company or organizationSeven Hills, OHPVGPATDIS, file of 2026-04-10

Inventors

InventorPlacePatentsPerson pageSource
Bassam AlnaslehParma Heights, OH4PVGPATDIS, file of 2026-04-10
Ching-Feng ChangStrongsville, OH13PVGPATDIS, file of 2026-04-10
Omer GulOlmsted Falls, OH9PVGPATDIS, file of 2026-04-10
Andrew Adam HausnerParma Heights, OH3PVGPATDIS, file of 2026-04-10
Robert E. MillerSouthaven, MS5PVGPATDIS, file of 2026-04-10
Orest L. AdrianowyczBroadview Heights, OH3PVGPATDIS, file of 2026-04-10

CPC categories

SubclassCategoryFirst groupSource
D01FChemical features in the manufacture of artificial filaments, threads, fibres, bristles or ribbons; apparatus specially adapted for the manufacture of carbon filamentsD01F9/17PVGPATDIS, file of 2026-04-10
C07GCompounds of unknown constitutionC07G1/00PVGPATDIS, file of 2026-04-10
C08HDerivatives of natural macromolecular compoundsC08H6/00PVGPATDIS, file of 2026-04-10
C08LCompositions of macromolecular compoundsC08L97/005PVGPATDIS, file of 2026-04-10

Cooperative Patent Classification, as currently assigned (one row per subclass).

Assignments and security interests

RecordedWhatFromToReel/frameSource
2024-12-23Security interest Security interest
Security interest
GRAFTECH INTERNATIONAL HOLDINGS INC. signed 2024-12-23U.S. BANKS TRUST COMPANY, NATIONAL ASSOCIATION EDISON, NJ72905/832ECORSEXC, file of 2026-09-25
2024-12-23Security interest Security interest
Security interest
GRAFTECH INTERNATIONAL HOLDINGS INC. signed 2024-12-23U.S. BANKS TRUST COMPANY, NATIONAL ASSOCIATION EDISON, NJ72905/497ECORSEXC, file of 2026-09-25
2024-12-23Release of security interest
Termination and release of patent security agreement (reel 054724 frame 0588 and 063798 frame 0928)
U.S. BANK TRUST COMPANY signed 2024-12-23GRAFTECH INTERNATIONAL HOLDINGS INC. BROOKLYN HEIGHTS, OH69762/518ECORSEXC, file of 2026-09-25
2024-12-23Release of security interest
Termination and release of patent security agreement (reel 064075 frame 0455)
U.S. BANK TRUST COMPANY signed 2024-12-23GRAFTECH INTERNATIONAL HOLDINGS INC. BROOKLYN HEIGHTS, OH69762/491ECORSEXC, file of 2026-09-25
2024-12-23Security interest Security interest
Security interest
GRAFTECH INTERNATIONAL HOLDINGS INC. signed 2024-12-23GLAS AMERICAS LLC JERSEY CITY, NJ69666/444ECORSEXC, file of 2026-09-25
2023-06-27Security interest Security interest
Security interest
GRAFTECH INTERNATIONAL HOLDINGS INC. signed 2023-06-26U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT CLEVELAND, OH64075/455ECORSEXC, file of 2026-09-25
2020-12-22Security interest Security interest
Security interest
GRAFTECH INTERNATIONAL HOLDINGS INC. signed 2020-12-22U.S. BANK NATIONAL ASSOCIATION, AS AGENT CLEVELAND, OH54724/588ECORSEXC, file of 2026-09-25
2018-02-12Security interest Security interest
Security interest
GRAFTECH INTERNATIONAL HOLDINGS INC. signed 2018-02-12JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT BROOKLYN, NY45308/591ECORSEXC, file of 2026-09-25
2018-02-12Release of security interest
Release of security interest
JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT signed 2018-02-12GRAFTECH INTERNATIONAL HOLDINGS INC. BROOKLYN HEIGHTS, OH45308/567ECORSEXC, file of 2026-09-25
2017-08-08Assignment
Assignment of assignor's interest
ALNASLEH, BASSAM signed 2013-11-01
HAUSNER, ANDREW signed 2015-06-16
ADRIANWYCZ, OREST L. signed 2015-06-17
CHANG, CHING-FENG signed 2015-06-30
GUL, OMER signed 2015-07-30
MILLER, ROBERT E. signed 2015-08-11
GRAFTECH INTERNATIONAL HOLDINGS INC. BROOKLYN HEIGHTS, OH43226/387ECORSEXC, file of 2026-09-25

Documents recorded with the USPTO Assignment Recordation Branch that list this patent. A security interest is a lender’s claim on the patent as collateral; a release ends it.

USPTO bulk data: PatentsView granted patents, disambiguated (PVGPATDIS) for patents, assignees, inventors, places and CPC categories; the USPTO Patent Assignment Dataset (ECORSEXC) for assignments and security interests. Patents filed in the last 20 years. No claims or full text. Links to other records are by name (and state): EXACT means the identical full name and state; FUZZY means a looser name match, with the confidence shown.